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/content/aip/journal/adva/5/6/10.1063/1.4923329
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/content/aip/journal/adva/5/6/10.1063/1.4923329
2015-06-26
2016-09-28

Abstract

A structural heterogeneity of the melt-spun FeSiBPCu alloy has been studied by spherical aberration () corrected high-resolution transmission electron microscopy. Hollow-cone illumination imaging revealed that the density of coherent scattering regions in the as-quenched FeSiBPCu alloy is much higher than that in the FeSiBP bulk metallic glass. According to the -corrected TEM, crystalline atomic clusters, typically of ∼1 nm in diameter, are densely distributed in an amorphous matrix of FeSiBPCu alloy. Observation of four-fold and six-fold atomic arrangements of these clusters implies existence of Fe clusters with the body centered cubic structure. These Fe clusters must be responsible for the formation of ultrahigh-density α-Fe nanocrystals produced by post-annealing.

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