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42.See supplementary material at http://dx.doi.org/10.1063/1.4930915 for [Representative SEM image of the Gp particles before the milling. (a) Representative SEM image and EDS mapping images of an iron particle milled for 0.10 h in the presence of Gp, where the particle’s C (b) and Fe (c) contents were mapped using EDS. Changes of the inner total pressure with the milling time for iron milled (solid line) with Gp and (broken line) without Gp. XRD patterns of different amounts of iron particles milled with (a) and without (b) Gp for 1.00 h. Pole figures of the (a) (110) and (b) (002) planes of the particles before the milling. Pole figures of the (a–c) (111), (002), and (022) planes of copper particles before and (d–f) after the milling. Possible mechanism by which the force imparted to the iron particle surface for the texture formation is controlled.].[Supplementary Material]
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/content/aip/journal/adva/5/9/10.1063/1.4930915
2015-09-09
2016-12-05

Abstract

Crystallographically anisotropic platelet iron particles were successfully prepared using a conventional ball mill with addition of graphite (Gp) particles. The morphological and structural changes resulting from the milling were investigated using scanning electron microscopy and X-ray diffraction. The spherical iron particles were plastically deformed into platelet shapes during the milling. Simultaneously, it is suggested that the size of the Gp particles decreased and adhered as nanoparticles on the surface of the iron particles. The adhered Gp particles affected the plastic deformation behavior of the iron particles: the {001} planes of α-iron were oriented parallel to the particle face, and no preferred in-plane orientation was observed. This study not only details the preparation of soft magnetic metal particles that crystallographically oriented to enhance their magnetic properties but also provides new insight into the activities of the well-established and extensively studied mechanical milling method.

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