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/content/aip/journal/adva/6/5/10.1063/1.4944656
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/content/aip/journal/adva/6/5/10.1063/1.4944656
2016-03-17
2016-09-28

Abstract

This work presents a study of how the magnetic and temperature variables, as well as the measurement rate, affect magnetic and structural phase transitions for LaCaSrMnO (x=0.15, 0.08, 0.07 and 0.06) manganites. A single phase rhombohedral crystal structure for Sr compound and a single phase orthorhombic crystal structure for Sr, Sr, and Sr compounds were identified by X ray diffraction. The Curie temperature adjustment to room temperature was reached for Sr sample, in which a Jahn-Tellertransition was observed. This Jahn-Tellertransition showed a susceptible response to 0.5, 1, 2, 3, 5 and 7 K/min measurement rates, and was revealed without measurement sequence at 234, 257, 196, 233, 245 and 238 K respectively in thermomagnetic curves (10mT). Also, Curie temperature increases sequentially around 2 K for the same measurement rates. To avoid magnetic field effect, a differential scanning calorimetry for Sr sample was obtained in the same temperature region, for 2, 3, 5, 7 K/min showing the Jahn-Teller phase transition at 225 K and a vibrational like behavior in the heat flux below 225 K, for all the temperature rates. The latter, is related to the static to dynamic Jahn-Tellertransition. Furthermore, Curie temperature appears around 284 K.

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