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Optical limiting behavior of a glass–ceramic containing sodium niobate crystallites
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8.For heat-treatment times varying from 0 to 8 h, the glass samples were translucent with minimal transparency after 4 h of heat treatment. X-ray diffraction, including SAXS measurements, proved that a liquid–liquid phase separation is the first step of glass crystallization and liquid drops resulting in strong light scattering are greatly reduced for heat treatment exceeding 8 h.
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