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Nanocrystals of cerium and europium trifluorides generated by coaxial Taylor cone electrospray of aqueous solutions at room temperature
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10.1063/1.1999840
/content/aip/journal/apl/87/5/10.1063/1.1999840
http://aip.metastore.ingenta.com/content/aip/journal/apl/87/5/10.1063/1.1999840

Figures

Image of FIG. 1.
FIG. 1.

Taylor’s double-cone electrospray scheme. Pressurized vessels are indicated showing the platinum wire used as electrical contact for the inner liquid.

Image of FIG. 2.
FIG. 2.

(a). HRTEM micrograph from a spherical particle. (b) Fast Fourier transform from the previous image indexed as the [001] -tysonite zone axis.

Image of FIG. 3.
FIG. 3.

(a). Transmission electron micrograph from a nanocrystal. (b) High resolution magnification from previous figure showing the microdomain constitution of the nanocrystal. (c) FFT obtained from the image of Fig. 2(a) indexed as two twins of tysonite along the [001] zone axis indicated by arrows and arrowheads. (d) Image reconstructed with all the first order reflections from the main twin. (e) Image reconstructed with all the first order reflections from the secondary twin. (f) Image reconstructed with only the 100 reflection pair of the main twin to show the mosaicity of the nanocrystal.

Tables

Generic image for table
Table I.

Lattice spacings measured by TEM observations compared with tysonite lattice spacings.

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/content/aip/journal/apl/87/5/10.1063/1.1999840
2005-07-26
2014-04-20
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752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: Nanocrystals of cerium and europium trifluorides generated by coaxial Taylor cone electrospray of aqueous solutions at room temperature
http://aip.metastore.ingenta.com/content/aip/journal/apl/87/5/10.1063/1.1999840
10.1063/1.1999840
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