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XPS of Sb spectra showing the progressive removal of oxide by thermal annealing under UHV conditions and by MHC; (a) as-loaded, (b) for , (b) for , and (c) MHC at under pressure of for .
AFM images taken after thermal annealing at various temperatures and after MHC: (a) as-loaded, (b) after at , and (c) after MHC for at a temperature of and a pressure of .
AE spectra measured upon MHC at for different period of times: (a) as loaded, (b) , (c) , and (d) .
Quantitative XPS analysis of the stoichiometry after thermal annealing at various temperatures and after MHC.
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