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In situ investigation of the liquid/solid interface of a block copolymer solution under shear stress using microbeam grazing-incidence small-angle x-ray scattering
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10.1063/1.2815929
/content/aip/journal/apl/91/21/10.1063/1.2815929
http://aip.metastore.ingenta.com/content/aip/journal/apl/91/21/10.1063/1.2815929
View: Figures

Figures

Image of FIG. 1.
FIG. 1.

(Color online) (a) Scheme of the experimental setup. X denotes the incoming x-ray beam and the incidence angle. (b) Change of the scattering pattern at with increasing shear rate ( , 5, 12, 55, 164, 208, 258, 360, and ). The dotted lines indicate the detector cuts shown in Fig. 2 .

Image of FIG. 2.
FIG. 2.

(a) Detector cuts of the interface signal at . The arrows show the position of the maximum. (b) Calculated spacings vs shear rate at different temperatures (inset: initial response for ).

Image of FIG. 3.
FIG. 3.

(Color online) Exaggerated sketch of the detachment (a) without shear the corona blocks of the micelles get attached to the metal surface (b) with shear the corona blocks are detached from the metal surface.

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/content/aip/journal/apl/91/21/10.1063/1.2815929
2007-11-19
2014-04-24
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752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: In situ investigation of the liquid/solid interface of a block copolymer solution under shear stress using microbeam grazing-incidence small-angle x-ray scattering
http://aip.metastore.ingenta.com/content/aip/journal/apl/91/21/10.1063/1.2815929
10.1063/1.2815929
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