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Resonant x-ray diffraction as a tool to calculate mixed valence ratios: Application to Prussian Blue materials
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10.1063/1.2952457
/content/aip/journal/apl/92/26/10.1063/1.2952457
http://aip.metastore.ingenta.com/content/aip/journal/apl/92/26/10.1063/1.2952457

Figures

Image of FIG. 1.
FIG. 1.

(a) Ratio of the normalized integrated intensities of the different wavelengths used, showing the effect on the various Bragg reflections. Dashed lines serve to guide the eyes. (b) Fe -edge absorption of the PB sample. The horizontal arrows indicate that two of the wavelengths ( and ) are outside the limits used for this measurement. The vertical arrow shows the position of the other wavelength .

Image of FIG. 2.
FIG. 2.

Rietveld refinements of the structure measured at two distinct wavelengths: (a) and (b) . (+) observed, (red line) calculated, (blue line) difference, and (magenta symbol) Bragg reflections. A few selected indexed reflections are indicated.

Image of FIG. 3.
FIG. 3.

Rietveld refinements (selected regions) of the structure measured at three distinct wavelengths: (a) , (b) , and (c) . (+) observed, (red line) calculated, (blue line) difference, and (magenta symbol) Bragg reflections. Various selected indexed reflections are indicated.

Tables

Generic image for table
Table I.

Integrated intensities, normalized with respect to the (200) one, of the three distinct wavelengths: , , and .

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/content/aip/journal/apl/92/26/10.1063/1.2952457
2008-07-02
2014-04-16
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752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: Resonant x-ray diffraction as a tool to calculate mixed valence ratios: Application to Prussian Blue materials
http://aip.metastore.ingenta.com/content/aip/journal/apl/92/26/10.1063/1.2952457
10.1063/1.2952457
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