1887
banner image
No data available.
Please log in to see this content.
You have no subscription access to this content.
No metrics data to plot.
The attempt to load metrics for this article has failed.
The attempt to plot a graph for these metrics has failed.
Direct observation of ion exchange in mechanically activated system using ultrahigh field nuclear magnetic resonance spectroscopy
Rent:
Rent this article for
USD
10.1063/1.3110966
/content/aip/journal/apl/94/14/10.1063/1.3110966
http://aip.metastore.ingenta.com/content/aip/journal/apl/94/14/10.1063/1.3110966
View: Figures

Figures

Image of FIG. 1.
FIG. 1.

MAS NMR spectra of (a) , (b) , (c) with 3 h ball milling, and (d) with 120 h ball milling. The spectra were obtained on about 5 mg of samples each with (a) 512, (b) 854, (c) 414, and (d) 1979 scans and a recycle delay time of 1 s. Spinning rates used were 16 kHz for (a), (c), and (d), while 10 kHz for (b). Peaks labeled by “” are spinning sidebands.

Image of FIG. 2.
FIG. 2.

(a) MAS NMR spectra: (i) , (ii) with 3 h ball milling, (iii) with 120 h ball milling. (b) MAS NMR spectra: (i) MgO, (ii) , (iii) with 120 h ball milling, (iv) with 3 h ball milling, and (v) . All the spectra were obtained on about 5 mg of samples each using a sample spinning rate of 16 kHz with (i) 16, (ii) 128, and (iii) 128 scans and a recycle delay time of 70 s for (a) samples and (i) 3800, (ii) 240 000, (iii) 83 000, (iv) 200 000, and (v) 30 000 scans and a recycle delay time of 0.2 s for (b) samples.

Image of FIG. 3.
FIG. 3.

Proposed structure changes (a) before and (b) after long-time ball milling.

Loading

Article metrics loading...

/content/aip/journal/apl/94/14/10.1063/1.3110966
2009-04-08
2014-04-23
Loading

Full text loading...

This is a required field
Please enter a valid email address
752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: Direct observation of ion exchange in mechanically activated LiH+MgB2 system using ultrahigh field nuclear magnetic resonance spectroscopy
http://aip.metastore.ingenta.com/content/aip/journal/apl/94/14/10.1063/1.3110966
10.1063/1.3110966
SEARCH_EXPAND_ITEM