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Measurement of heat capacity and enthalpy of formation of nickel silicide using nanocalorimetry
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10.1063/1.3255009
/content/aip/journal/apl/95/18/10.1063/1.3255009
http://aip.metastore.ingenta.com/content/aip/journal/apl/95/18/10.1063/1.3255009
View: Figures

Figures

Image of FIG. 1.
FIG. 1.

(a) Temperature profile. (b) Heating rate. (c) Heat capacities of the sensor and film at various stages of the experiment after accounting for heat loss. The top green line (Standard DSC) is from a conventional DSC (scan rate: ). Due to the small sample volume, the conventional DSC measurement is considered as arbitrary units for qualitative comparison; (b) the reaction peak—. (e) Derivative of the peak which shows three distinct inflection points.

Image of FIG. 2.
FIG. 2.

(a) Indexed EBSD pattern corresponding to the phase found in the sample heated to . (b) Indexed EBSD pattern of the NiSi phase found in sample heated to . (c) Heat capacity results from a sample that was heated to a lower temperature ( in the first pulse) and (d) the indexed EBSD pattern of the end product (NiSi) of this experiment. (e), (f) Grain structure of the reaction products of sample heated to .

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/content/aip/journal/apl/95/18/10.1063/1.3255009
2009-11-05
2014-04-25
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752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: Measurement of heat capacity and enthalpy of formation of nickel silicide using nanocalorimetry
http://aip.metastore.ingenta.com/content/aip/journal/apl/95/18/10.1063/1.3255009
10.1063/1.3255009
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