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Electric field assisted dissolution of Au rods in gold-doped silicate glass
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View: Figures


Image of FIG. 1.
FIG. 1.

Experimental setup for electric field thermal poling. (1) Tube furnace, (2) thermal couple, (3) dc power, (4) anode, (5) steel plate, (6) sample, (7) BN carrier, and (8) steel rod holder as cathode (fixed on 5).

Image of FIG. 2.
FIG. 2.

Optical and SEM images of the as-poled sample. (1) Photograph of the sample near the edge of anode after EFAD. The three zones in (1) are denoted as zone A (far away from the anode), zone B (the transition region), and zone C (just below the anode), whose locally selected SEM images are shown in (2), (3), (4), and (5), respectively.

Image of FIG. 3.
FIG. 3.

Absorption spectra of Au-doped silicate glass before (a) and after (b) annealing at without an electric field.

Image of FIG. 4.
FIG. 4.

Absorption spectra for the three different zones A, B, and C of the as-poled sample.

Image of FIG. 5.
FIG. 5.

Evolution of applied current and voltage as a function of time during electric field thermal poling.

Image of FIG. 6.
FIG. 6.

Conduction current evolution with dissolution time at 800 V during electric field thermal poling.


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752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: Electric field assisted dissolution of Au rods in gold-doped silicate glass