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From to nanostructured sisal-like and CuO: Synthesis and characterization
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10.1063/1.3097286
/content/aip/journal/jap/105/6/10.1063/1.3097286
http://aip.metastore.ingenta.com/content/aip/journal/jap/105/6/10.1063/1.3097286
View: Figures

Figures

Image of FIG. 1.
FIG. 1.

The XRD patterns of (a) samples, (b) the samples after NaOH treatment , and (c) CuO products and the corresponding EDX element analysis (inset).

Image of FIG. 2.
FIG. 2.

Typical SEM images of the as-prepared samples. (a) The octahedral . (b) The sisal-like . (c) Low magnification of the sisal-like CuO. (d) High magnification of the nanoneedles of CuO.

Image of FIG. 3.
FIG. 3.

[(a)–(d)] The time-dependent optical images during the octahedral was treated with NaOH solution. [(e)–(f)] SEM images taken for samples collected at different reaction times.

Image of FIG. 4.
FIG. 4.

A schematic of the proposed mechanism for overall transformation.

Image of FIG. 5.
FIG. 5.

(a) UV-vis absorption spectrum of the sisal-like CuO. (b) vs curves of the products.

Image of FIG. 6.
FIG. 6.

(a) Wide X-ray photoelectron spectrum of the as-prepared CuO. [(b) and (c)] High-resolution XPS spectra for the and regions, respectively.

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/content/aip/journal/jap/105/6/10.1063/1.3097286
2009-03-24
2014-04-18
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752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: From Cu2(OH)3Cl to nanostructured sisal-like Cu(OH)2 and CuO: Synthesis and characterization
http://aip.metastore.ingenta.com/content/aip/journal/jap/105/6/10.1063/1.3097286
10.1063/1.3097286
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