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Correlation of electron backscatter diffraction and piezoresponse force microscopy for the nanoscale characterization of ferroelectric domains in polycrystalline lead zirconate titanate
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10.1063/1.3474940
/content/aip/journal/jap/108/4/10.1063/1.3474940
http://aip.metastore.ingenta.com/content/aip/journal/jap/108/4/10.1063/1.3474940
View: Figures

Figures

Image of FIG. 1.
FIG. 1.

Secondary electron SEM image of the PZT polished and etched surface. Grains and ferroelectric domains are clearly resolved.

Image of FIG. 2.
FIG. 2.

The region selected for subsequent analysis: (a) SEM image with the EBSD scan area marked in red and (b) EBSD orientation map. The legend line shows the location of the orientation profile shown in Fig. 3.

Image of FIG. 3.
FIG. 3.

Line-scan of the relative crystallographic orientations measured using EBSD across the legend line in Fig. 2(b).

Image of FIG. 4.
FIG. 4.

PFM images of the area depicted in Fig. 2. (a) SEM image, (b) AFM topography, and (c) PFM amplitude.

Image of FIG. 5.
FIG. 5.

Line scans of the piezoresponse for two adjacent regions A and B (a) line scan locations and (b) PFM amplitude along the line scan.

Image of FIG. 6.
FIG. 6.

Values of the piezoresponse peaks from Fig. 5.

Image of FIG. 7.
FIG. 7.

Vertical piezoresponse amplitude calculated from the EBSD map.

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/content/aip/journal/jap/108/4/10.1063/1.3474940
2010-08-31
2014-04-19
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752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: Correlation of electron backscatter diffraction and piezoresponse force microscopy for the nanoscale characterization of ferroelectric domains in polycrystalline lead zirconate titanate
http://aip.metastore.ingenta.com/content/aip/journal/jap/108/4/10.1063/1.3474940
10.1063/1.3474940
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