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Synthesis and pore filling mechanism in anatase TiO2 nanostructured network mediated by PbS molecular adsorption
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10.1063/1.3583648
/content/aip/journal/jap/109/9/10.1063/1.3583648
http://aip.metastore.ingenta.com/content/aip/journal/jap/109/9/10.1063/1.3583648
View: Figures

Figures

Image of FIG. 1.
FIG. 1.

(Color online) XRD patterns of the (a) nanostructured TiO2 and (b) PbS/TiO2 systems. The respective Williamson–Hall plots of the TiO2 and PbS/TiO2 systems are shown on the right.

Image of FIG. 2.
FIG. 2.

SEM micrographs of the (a) nanostructured TiO2 and (b) PbS/TiO2 systems. A TEM image depicting PbS nanoparticles located on the nanostructured surface of TiO2 is shown in (c).

Image of FIG. 3.
FIG. 3.

(Color online) EDX patterns of the (a) nanostructured TiO2 and (b) PbS/TiO2 systems.

Image of FIG. 4.
FIG. 4.

(Color online) AFM surface topology of the (a) nanostructured TiO2 and (b) PbS/TiO2 systems.

Image of FIG. 5.
FIG. 5.

Comparison of pore size distribution vs N2 desorption for the (a) nanostructured TiO2 and (b) PbS/TiO2 systems.

Image of FIG. 6.
FIG. 6.

Surface area comparison of (a) untreated TiO2 and (b) the PbS adsorbed TiO2 system.

Image of FIG. 7.
FIG. 7.

N2 adsorption isotherms of (a) untreated TiO2 and (b) the PbS adsorbed TiO2 system.

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/content/aip/journal/jap/109/9/10.1063/1.3583648
2011-05-10
2014-04-23
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752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: Synthesis and pore filling mechanism in anatase TiO2 nanostructured network mediated by PbS molecular adsorption
http://aip.metastore.ingenta.com/content/aip/journal/jap/109/9/10.1063/1.3583648
10.1063/1.3583648
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