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Radical modification of the wetting behavior of textiles coated with ZnO thin films and nanoparticles when changing the ambient pressure in the pulsed laser deposition process
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10.1063/1.3639297
/content/aip/journal/jap/110/6/10.1063/1.3639297
http://aip.metastore.ingenta.com/content/aip/journal/jap/110/6/10.1063/1.3639297

Figures

Image of FIG. 1.
FIG. 1.

(Color online) Textile material partially coated with ZnO nanostructures: (a) hydrophilic TF deposited in a 13 Pa oxygen flux, (b) hydrophobic TF deposited in vacuum, and (c) hydrophobic NP deposited in vacuum. Images were acquired with a CANON EOS 50 D digital camera.

Image of FIG. 2.
FIG. 2.

SEM micrograph of the superhydrophobic textile coated with ZnO TF in vacuum, at a target-to-substrate separation distance of d = 5 cm. Inset: Water droplet in static mode with the CA of 157°.

Image of FIG. 3.
FIG. 3.

SEM micrograph of the textile sputtered with NP. Inset: Water droplet in static mode with a CA of 120°.

Image of FIG. 4.
FIG. 4.

Textile material fibers coated with ZnO: (a) NP deposited by PLD with 10 pulses, (b) TF deposited by PLD with 100 pulses.

Image of FIG. 5.
FIG. 5.

2D AFM topography images for the TF deposited in (a),(c) a 13 Pa oxygen flux and (b),(d) vacuum at different scales: (a),(b) (10 × 10) μm2 and (c),(d) (2 × 2) μm2.

Image of FIG. 6.
FIG. 6.

SEM micrographs of ZnO NP deposited in a 13 Pa oxygen flux on a Si substrate. Target-substrate separation distance was of (a) 3 cm, (b) 4 cm, and (c) 5 cm. Inset: Water droplet in static mode and the measured CA.

Image of FIG. 7.
FIG. 7.

XRD patterns for ZnO TF deposited onto: (A) silicon substrate and (B) textile substrate. Rocking curves (ω scans) for the involved crystal planes: (b) (002), (c) (101), (d) (100), and (e) (110).

Image of FIG. 8.
FIG. 8.

(Color online) ZnO lattice with the crystal planes parallel to the surface in the ZnO films synthesized in an oxygen flux (a)-(001) and (101) planes containing a single type of atoms, and in the ZnO films synthesized in vacuum, (b)-(100) and (110) planes consisting of pairs of Zn plus O atoms.

Image of FIG. 9.
FIG. 9.

(Color online) Plasma plume in PLD recorded in 13 Pa oxygen flux (a) and vacuum (b).

Image of FIG. 10.
FIG. 10.

(Color online) Schematic of the water droplet in contact with ZnO surface deposited in vacuum (a) and in a 13 Pa oxygen flux (b).

Tables

Generic image for table
Table I.

Amplitude parameters RMS, Ssk and Sku for ZnO TF deposited in 13 Pa oxygen flux or vacuum.

Generic image for table
Table II.

NP size and density on Si substrate.

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/content/aip/journal/jap/110/6/10.1063/1.3639297
2011-09-26
2014-04-25
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752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: Radical modification of the wetting behavior of textiles coated with ZnO thin films and nanoparticles when changing the ambient pressure in the pulsed laser deposition process
http://aip.metastore.ingenta.com/content/aip/journal/jap/110/6/10.1063/1.3639297
10.1063/1.3639297
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