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Electron spin resonance identification of a methyl associated organic radical in irradiated amorphous SiO2
1.Wm. R. Austin and R. G. Leisure, Phys. Rev. B. (accepted for publication).
2.D. L. Griscom, M. Stapelbroek, and E. J. Friebele, J. Chem. Phys. 78, 1638 (1983).
3.J. H. Stathis and M. A. Kastner, Phys. Rev. B 29, 7079 (1984).
4.E. J. Friebele, D. L. Griscom, and K. Rau, J. Non-Cryst. Solids 57, 167 (1983).
5.M. C. R. Symons, in Advances in Physical Organic Chemistry, edited by V. Gold (Academic, New York, 1963), Vol. 1, pp. 284–363, and references therein.
6.Samples provided courtesy of Dr. Thomas Seward, Corning Inc. Corning 7940 is a trade name of Corning Inc., Corning, NY.
7.Samples purchased from Heraeus Amersil Inc. Suprasil 1 and Suprasil W1 are trade names of Heraeus Amersil Inc., Buford, GA.
8.G. W. Arnold and W. D. Compton, Phys. Rev. 116, 802 (1959).
9.The signal is phase inverted in the spectra of Figs. 1 and 2(a);
9.this is an instrumentation effect associated with saturation of the center at high microwave power.
10.D. L. Griscom, J. Ceram. Soc. Jpn. 99, 923 (1991), and references therein.
11.R. A. Weeks and C. M. Nelson, J. Appl. Phys. 31, 1555 (1960).
12.F. L. Galeener, D. B. Kerwin, and A. J. Miller, Phys. Rev. B. 47, 7760 (1993), and references therein.
13.M. Stapelbroek, D. L. Griscom, E. J. Friebele, and G. H. Sigel, Jr., J. Non-Cryst. Solids 32, 313 (1979).
14.E. J. Friebele, D. L. Griscom, M. Stapelbroek, and R. A. Weeks, Phys. Rev. Lett. 42, 1346 (1979).
15.Wm. R. Austin and R. G. Leisure (unpublished data).
16.D. L. Griscom, Nucl. Instrum. Methods Phys. Res. B 46, 12 (1990).
17.Lin Zhang, V. A. Mashkov, and R. G. Leisure, Phys. Rev. B 53, 7182 (1996).
18.Wm. R. Austin and R. G. Leisure (unpublished data). Previous observation of the peroxy radical (“dry“ OHC) in Suprasil 1 is reported by: D. L. Griscom, J. Non-Cryst. Solids 31, 241 (1978).
19.Presuming diffusivity trends in opposition to molecular size. In the network at room temperature diffuses readily and marginally (time scale of hours to days) while is essentially trapped. A review of experimental evidence regarding diffusion and radiation kinetics in is presented by D. L. Griscom in SPIE Vol. 541 - Radiation Effects in Optical Materials, (Society of Photo-Optical Instrumentation Engineers, Bellingham, WA, 1985), pp. 38–59.
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