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Schematic of the experimental setup.
Schematics of the copper holder support (left) and cross section of the twin membrane-based nanocalorimeter system (right).
Heat capacity curves obtained from the first scan after film deposition of the various glass forming liquids as a function of temperature. Curves are smoothed for clarity with a ten point adjacent averaging.
Heat capacity of a toluene film (nominal thickness of around 40 nm) obtained by averaging 50 consecutive measurements under identical heating and cooling conditions.
Differential voltage vs temperature for glassy films of acetic acid analyzed at various heating rates.
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