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IUPAC-NIST Solubility Data Series. 84. Solubility of Inorganic Actinide Compounds
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Figures

Image of FIG. 1.
FIG. 1.

Solubility of in aqueous NaF solutions.

Image of FIG. 2.
FIG. 2.

Solubility of in aqueous solutions.

Image of FIG. 3.
FIG. 3.

Selected literature data for the solubility of crystalline (references in Fig. 3 are as follows: 1, Zhidikova et al.,343 2, Moon,184 3, Rai et al.,251 and 4, Neck et al. 206).

Image of FIG. 4.
FIG. 4.

Literature data for the solubility of microcrystalline (references in Fig. 4 are as follows: 3, Rai et al.,251 4, Neck and Kim,204 6, Baes et al.,24 and 7, Bundschuh et al. 42).

Image of FIG. 5.
FIG. 5.

Thorium oxide or thorium oxide hydrate–sodium perchlorate–water system.

Image of FIG. 6.
FIG. 6.

Comparison of literature data on the solubility of amorphous (references in Fig. 6 are as follows: 2, Rai et al.,251 4, Bundschuh et al.,42 5, Ryan and Rai,268 7, Nabivanets and Kudritskaya,198 10, Rai et al.,248 11, Neck et al.,208 12, Bilinski et al.,31 and 13, Gayer and Leider107).

Image of FIG. 7.
FIG. 7.

Thorium oxide hydrate–sodium chloride–water system.

Image of FIG. 8.
FIG. 8.

Thorium oxide hydrate–magnesium chloride–water system.

Image of FIG. 9.
FIG. 9.

Thorium oxide hydrate-sodium perchlorate-water system (legend: triangles, series 1; squares, series 2, circles, series 3, arrows tips, detection limits in series 1 solutions).

Image of FIG. 10.
FIG. 10.

Thorium oxide hydrate-sodium carbonate-water system.

Image of FIG. 11.
FIG. 11.

Thorium oxide hydrate-sodium hydroxide-sodium carbonate-water system.

Image of FIG. 12.
FIG. 12.

Thorium oxide hydrate-sodium hydrogen carbonate-water system.

Image of FIG. 13.
FIG. 13.

Thorium oxide hydrate-sodium silicate-sodium perchlorate-water system (squares: ; circles: ; triangles: not clear from the original document).

Image of FIG. 14.
FIG. 14.

Thorium sulfate-water system.[Crosses with numbers pointing to them refer to and other symbols to or . References in Fig. 14 are as follows: 2, Demarcay;68 3, Roozeboom;263 4, Cleve;58 5, Wyrouboff;336 6, Wirth;335 and 7, Khuan-Ban and Fedorov.130].

Image of FIG. 15.
FIG. 15.

Thorium diphosphate-hydrogen chloride-water system.

Image of FIG. 16.
FIG. 16.

Thorium diphosphate-acids-water system.

Image of FIG. 17.
FIG. 17.

Thorium phosphate diphosphate-sodium perchlorate-water system (method of analysis: open circles, PERALS, full circles, ICP-MS, squares, PIXE).

Image of FIG. 18.
FIG. 18.

Uranium hexafluoride-tungsten hexafluoride system (full circles: differential thermography; open circles: polythermal method).

Image of FIG. 19.
FIG. 19.

Uranium hexafluoride-halogenated solvent system (solvent: 1, ; 2, ; 3, ; 4, ; 5, ; 6, ; 7, ; 8, ; 9, ).

Image of FIG. 20.
FIG. 20.

Dioxouranium (VI) fluoride-water system.

Image of FIG. 21.
FIG. 21.

Uranium (VI) oxide-hydrogen fluoride-water system.

Image of FIG. 22.
FIG. 22.

Dioxouranium (VI) fluoride-acetone-water system (fields: A, unsaturated solutions; B, saturated ; C, saturated ; D, saturated ).

Image of FIG. 23.
FIG. 23.

Ammonium pentafluorobis(dioxouranate (VI))-ammonium fluoride-water system.

Image of FIG. 24.
FIG. 24.

Ammonium octafluorouranate(VI)-ammonium fluoride-water system.

Image of FIG. 25.
FIG. 25.

Uranium (IV) chloride-water system (adapted from the original document).

Image of FIG. 26.
FIG. 26.

Uranium (VI) oxide-hydrogen chloride-water system (solid phases: , [13867-67-9]; or (Kraus), congruently soluble; , [42861-14-3], identical with (Kraus), incongruently soluble; , [42861-14-3], metastable, incongruently soluble; , [20593-39-9]).

Image of FIG. 27.
FIG. 27.

Dioxouranium (VI) chloride-diethyl ether-water system (A: two liquid phases; B and C: homogeneous unsaturated aqueous and etheral solutions, respectively; D: saturated aqueous , [13867-67-9]; E: saturated aqueous ; F: saturated aqueous and etheral ; G: saturated etheral ; H: saturated ; I: saturated ; J: saturated etheral ).

Image of FIG. 28.
FIG. 28.

Solubility of .

Image of FIG. 29.
FIG. 29.

Solubility of .

Image of FIG. 30.
FIG. 30.

Cesium hexachlorouranate(IV)-methanol/acetonitrile/acetone-cesium chloride-water system (Curves: 1, methanol; 2, acetone; 3, acetonitrile).

Image of FIG. 31.
FIG. 31.

Dioxouranium (VI) perchlorate-diethyl ether-water system (also reported in Vdovenko et al. 329 [I: two liquid phases; II: homogeneous solutions; III: saturated ; IV: saturated solution ; V: saturated ; VI: saturated ].

Image of FIG. 32.
FIG. 32.

Dioxouranium (VI) perhlorate-di--butyl ether-water system (the diagram was also reported in Vdovenko et al. 339 [I: two liquid phases; II and X: homogeneous aqueous and etheral solutions, respectively; III: saturated aqueous and etheral ; IV: saturated etheral ; V: saturated ; VI and VII: saturated ; VIII: saturated ; IX: saturated ].

Image of FIG. 33.
FIG. 33.

Crystalline uranium (VI) oxide-perchlorate or chloride-water system (references are as follows: 1, Parks and Pohl;229 2, Torrero et al.;321 3, Yajima et al.;337 5, Rai et al. 258).

Image of FIG. 34.
FIG. 34.

Uranium (IV) oxide or uranium (IV) oxide hydrate-sodium perchlorate-sodium dithionite-water system [black symbols: undersaturation experiments with crystalline ; open symbols: oversaturation experiments with amorphous .]

Image of FIG. 35.
FIG. 35.

Uranium (IV) oxide hydrate-lithium hydroxide-water system (a) as a function of temperature and (b) at two LiOH concentrations at . Different symbols refer to different flow-system configurations. Blank measurements did not exceed U.

Image of FIG. 36.
FIG. 36.

Uranium (IV) oxide hydrate-europium (II) chloride-water system.

Image of FIG. 37.
FIG. 37.

Uranium (IV) oxide hydrate-sodium perchlorate water system.

Image of FIG. 38.
FIG. 38.

Uranium (IV) oxide hydrate-sodium chloride-water system.17

Image of FIG. 39.
FIG. 39.

Uranium (IV) oxide hydrate-sodium chloride-water system.248

Image of FIG. 40.
FIG. 40.

Uranium (IV) oxide hydrate-magnesium sodium chloride-water system.248

Image of FIG. 41.
FIG. 41.

Solubility of as a function of concentration in the presence of NaOH.

Image of FIG. 42.
FIG. 42.

Solubility of as a function of NaOH concentration in the presence of constant concentrations of or .

Image of FIG. 43.
FIG. 43.

Solubility of as a function of concentration.

Image of FIG. 44.
FIG. 44.

Phase diagram of the uranium(VI) oxide-nitric acid-water system. Scale in the graph not reported. Full circles: data from Kraus [C. A. Kraus, Brown University (1944); quoted in J. J. Katz and E. Rabinowitch, The Chemistry of Uranium (McGraw-Hill, New York 1951), p. 329], included by the authors. This source was not available to the compiler.

Image of FIG. 45.
FIG. 45.

The solubility of uranium(VI) oxide in nitric acid solutions as a function of temperature.

Image of FIG. 46.
FIG. 46.

Phase diagram of the system at . Full circles: data from Kraus, included by the author. This source was not available to the compiler; the source is C. A. Kraus, Brown University (1944); quoted in J. J. Katz and E. Rabinowitch, The Chemistry of Uranium (McGraw-Hill, New York, 1951), p. 329.

Image of FIG. 47.
FIG. 47.

Solubility of in aqueous solutions of at 20 and (open circles, measurements at ; full triangles, measurements at ; full circles, data from Lacher [J. Lacher, Inorg. Chem. 1, 4 (1962)]; open triangles, data from Cordfunke,62 data from Lacher and Cordfunke included by the authors).

Image of FIG. 48.
FIG. 48.

Comparison of selected data for the solubility of in weakly acidic to neutral solutions; Ref. 1 (Bruno and Sandino38), Ref. 5 (Nikitin et al. 20), Ref. 8 (Kramer-Schnabel et al. 146), Ref. 9 (Meinrath and Kimura171), Ref. 10 (Kato et al. 127), Ref. 11 (Gayer and Leider108), and Ref. 12 (Torrero et al. 320).

Image of FIG. 49.
FIG. 49.

Solubility of amorphous .

Image of FIG. 50.
FIG. 50.

Solubility of microcrystalline .

Image of FIG. 51.
FIG. 51.

Solubility of in at .

Image of FIG. 52.
FIG. 52.

The solubility of as a function of in solution at .

Image of FIG. 53.
FIG. 53.

The solubility of schoepite, referred to as , [20593-39-9], at . Square symbols, undersaturation measurements, circle symbols, oversaturation measurements; filled symbols, U concentrations measured after 14 and , respectively, for the under- and oversaturation experiments; open symbols, U concentrations measured between 14 and . Solid line, solubility of (schoepite) at calculated by the authors using the thermodynamic data from Langmuir [D. Langmuir, Geochim. Cosmochim. Acta 42, 547 (1978)] and considering the following U(VI) solution species [R. L. Lemire and P. R. Tremaine, J. Chem. Eng. Data 25, 361 (1980); R. N. Sylva and M. R. Davidson, J. Chem. Soc. Dalton Trans. 1979, 465]: , , , , , , , and .

Image of FIG. 54.
FIG. 54.

The solubility of (schoepite) in NaCl.

Image of FIG. 55.
FIG. 55.

The solubility of (compreignacite) in solution of KCl. (Initial solid phase: open circles, schoepite; full circles, compreignacite.)

Image of FIG. 56.
FIG. 56.

The solubility of (becquerelite) in solution of . (Initial solid phase: open circles, schoepite; full circles, becquerelite.)

Image of FIG. 57.
FIG. 57.

Phase diagram of the system below (Secoy277).

Image of FIG. 58.
FIG. 58.

Phase diagram of the system at and above (Secoy278).

Image of FIG. 59.
FIG. 59.

Phase diagrams of the and systems at . Solid phases: I: , [12415-63-4]; II: , [19126-66-0]; III. , [; IV: , [; V: ; VI: , [20593-39-9].

Image of FIG. 60.
FIG. 60.

Phase diagram of the system at .

Image of FIG. 61.
FIG. 61.

Solubility isotherm of the system at .

Image of FIG. 62.
FIG. 62.

Phase diagram of the system at .

Image of FIG. 63.
FIG. 63.

Phase diagram of the system at .

Image of FIG. 64.
FIG. 64.

Phase diagram of the system at .

Image of FIG. 65.
FIG. 65.

Phase diagram of the system at .

Image of FIG. 66.
FIG. 66.

Phase diagram of the system at .

Image of FIG. 67.
FIG. 67.

Phase diagram of the system at .

Image of FIG. 68.
FIG. 68.

Phase diagram of the system at .

Image of FIG. 69.
FIG. 69.

Solubility of in solutions of phosphoric acid.

Image of FIG. 70.
FIG. 70.

Phase diagram of the system at .

Image of FIG. 71.
FIG. 71.

Solubility of in solutions at .

Image of FIG. 72.
FIG. 72.

Solubility of U(VI) phosphates in solutions.

Image of FIG. 73.
FIG. 73.

Isothermal phase diagram of the system at .

Image of FIG. 74.
FIG. 74.

Solubility of in solutions of ionic strength of at .

Image of FIG. 75.
FIG. 75.

The solubility of was determined in water-solvent mixtures. Curves: 1, methanol; 2, acetone; 3, acetonitrile.

Image of FIG. 76.
FIG. 76.

Solubility of .

Image of FIG. 77.
FIG. 77.

Solubility of .

Image of FIG. 78.
FIG. 78.

Solubility of in carbonate-free water.

Image of FIG. 79.
FIG. 79.

Concentration of Np(IV) in solution saturated with amorphous as a function of KOH concentration.

Image of FIG. 80.
FIG. 80.

Concentration of Np(IV) in KOH solution saturated with amorphous as a function of concentration.

Image of FIG. 81.
FIG. 81.

Concentration of Np(IV) in solutions saturated with amorphous .

Image of FIG. 82.
FIG. 82.

Solubility of in concrete-preequilibrated water as a function of (points: experimental data, solid line: calculated values).

Image of FIG. 83.
FIG. 83.

Solubility of .

Image of FIG. 84.
FIG. 84.

Solubility of in solution.

Image of FIG. 85.
FIG. 85.

Solubility of in carbonate-free solutions at . Ionic strength (, ): (a) 0.1, amorphous ; (b) 1.0; (c) 3.0, aged .

Image of FIG. 86.
FIG. 86.

Solubility of in at .

Image of FIG. 87.
FIG. 87.

Solubility of as a function of in .

Image of FIG. 88.
FIG. 88.

Solubility of in water-solvent mixtures containing CsCl and HCl. Curves: 1, methanol; 2, acetone; 3, acetonitrile.

Image of FIG. 89.
FIG. 89.

Solubility of . in aqueous solutions of HCl.

Image of FIG. 90.
FIG. 90.

Solubility of . in aqueous solutions of HCl.

Image of FIG. 91.
FIG. 91.

Solubility of in water as a function of .

Image of FIG. 92.
FIG. 92.

Plutonium(IV) oxide hydrate-water system. (References are as follows: 3, Efurd et al.;82 4, Perez-Bustamante;237 5, Kim and Kanellakopulos;132 6, Fujiwara et al.;97 7, Nitsche and Edelstein;217 8, Pazukhin and Kudryavtsev;232 10, Rothe et al.;265 11, Ewart et al.;84 12, Rai et al.;254 13, Rai;241).

Image of FIG. 93.
FIG. 93.

Solubility of in concrete-preequilibrated water as a function of (points: experimental data, solid line: calculated values).

Image of FIG. 94.
FIG. 94.

Solubility of colloidal as a function of . A (left), ; B (right), . Circles: data obtained with -adjusted polymer, equilibrium attained from oversaturation direction; triangles: data obtained with flocculated polymer, equilibrium attained from undersaturation direction. Dotted lines represent the solubility of crystalline or amorphous as determined in the author’s earlier paper [D. Rai, R. J. Serne, and D. A. Moore, Soil Sci. Soc. Am. J. 44, 490 (1980)]. The numbers adjacent to points denote equilibration time in days.

Image of FIG. 95.
FIG. 95.

Solubility of as a function of the concentration of (open symbols) or ion (black symbols). The curves show the results of least squares fitting.

Image of FIG. 96.
FIG. 96.

Solubility of in solution.

Image of FIG. 97.
FIG. 97.

Solubility of and in solution. Solid lines were calculated by the authors from the equations or for or as the solid phases, respectively. Here [Am] and are the total americium concentration in solution dissolved from or , respectively, and is the dissolution constant for . The dissolution of was described by the authors to proceed according to the equation .

Image of FIG. 98.
FIG. 98.

Solubility of americium hydroxide, , as a function of (specific activity of : full circles, ; open circles, .)

Image of FIG. 99.
FIG. 99.

Solubility of americium hydroxide, , as a function of .

Image of FIG. 100.
FIG. 100.

Solubility of [and ] in concrete-preequilibrated water as a function of (solid line: calculated values from fit to experimental points).

Image of FIG. 101.
FIG. 101.

Solubility of amorphous as a function of .

Image of FIG. 102.
FIG. 102.

Solubility of in NaCl solution.

Image of FIG. 103.
FIG. 103.

Solubility of in NaCl solution.

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Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table
Generic image for table