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A high-pressure cell for kinetic studies on gas hydrates by powder x-ray diffraction
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10.1063/1.3520465
/content/aip/journal/rsi/81/12/10.1063/1.3520465
http://aip.metastore.ingenta.com/content/aip/journal/rsi/81/12/10.1063/1.3520465
View: Figures

Figures

Image of FIG. 1.
FIG. 1.

(Color online) Sketch of the pressure cell from (a) top view and (b) side view.

Image of FIG. 2.
FIG. 2.

(Color online) Photograph of the pressure cell mounted on the XYZ stage of the diffractometer.

Image of FIG. 3.
FIG. 3.

(Color online) GADDS image with 2θ versus intensity plot of a structure II CH4 + iso-C4H10 gas hydrate.

Image of FIG. 4.
FIG. 4.

(Color online) Powder x-ray diffractograms as a function of time collected during CH4 + iso-C4H10 hydrate formation from ice at one measuring point at 267 K and 1.06 MPa.

Image of FIG. 5.
FIG. 5.

Mean intensity ratio I/I 0 as a function of time during CH4 + iso-C4H10 hydrate formation from ice at 267 K and 1.06 MPa.

Image of FIG. 6.
FIG. 6.

(Color online) Intensity ratio I/I 0 as function of time during CO2 hydrate formation. In order to show the reproducibility of the experimental setup, three experiments were conducted under the same conditions: 267 K and 1.16 MPa.

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/content/aip/journal/rsi/81/12/10.1063/1.3520465
2010-12-22
2014-04-21
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752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: A high-pressure cell for kinetic studies on gas hydrates by powder x-ray diffraction
http://aip.metastore.ingenta.com/content/aip/journal/rsi/81/12/10.1063/1.3520465
10.1063/1.3520465
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