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Application of a new composite cubic-boron nitride gasket assembly for high pressure inelastic x-ray scattering studies of carbon related materials
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10.1063/1.3607994
/content/aip/journal/rsi/82/7/10.1063/1.3607994
http://aip.metastore.ingenta.com/content/aip/journal/rsi/82/7/10.1063/1.3607994
View: Figures

Figures

Image of FIG. 1.
FIG. 1.

Schematic diagram showing steps for making gasket assembly and sample loading [(a)–(d)].

Image of FIG. 2.
FIG. 2.

The photographs taken during the gasket preparation. A diamond anvil used for the gasket preparation and high pressure experiments (a), the as prepared c-BN disk on top of the diamond anvil (b), a c-BN insert ring with an outer diameter of 260 μm and an inner diameter of ∼80 μm (c), and the assembly of the c-BN insert ring and the Be gasket (d). The circle in (d) shows the boundary between the c-BN insert and the gasket.

Image of FIG. 3.
FIG. 3.

The 2D x-ray absorption map of the diamond tips, gasket, and sample (a), and the x-ray intensity along the line shown in Fig. 2(a) (b).

Image of FIG. 4.
FIG. 4.

IXS spectra of the solvated C60 sample at high pressure. The beam size is 10 μm × 40 μm (vertical × horizontal) at the sample location. The step size is 1 eV.

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/content/aip/journal/rsi/82/7/10.1063/1.3607994
2011-07-13
2014-04-17
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752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: Application of a new composite cubic-boron nitride gasket assembly for high pressure inelastic x-ray scattering studies of carbon related materials
http://aip.metastore.ingenta.com/content/aip/journal/rsi/82/7/10.1063/1.3607994
10.1063/1.3607994
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