Schematic diagram showing steps for making gasket assembly and sample loading [(a)–(d)].
The photographs taken during the gasket preparation. A diamond anvil used for the gasket preparation and high pressure experiments (a), the as prepared c-BN disk on top of the diamond anvil (b), a c-BN insert ring with an outer diameter of 260 μm and an inner diameter of ∼80 μm (c), and the assembly of the c-BN insert ring and the Be gasket (d). The circle in (d) shows the boundary between the c-BN insert and the gasket.
The 2D x-ray absorption map of the diamond tips, gasket, and sample (a), and the x-ray intensity along the line shown in Fig. 2(a) (b).
IXS spectra of the solvated C60 sample at high pressure. The beam size is 10 μm × 40 μm (vertical × horizontal) at the sample location. The step size is 1 eV.
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