- Conference date: 12–16 September 2010
- Location: Leipzig, (Germany)
Pulsed field gradient (PFG) and magic angle spinning (MAS) NMR techniques have been successfully combined for the study of mixture diffusion in porous materials. Using a modular setup of commercially available components, gradient pulses of up to can be applied coinciding with fast sample rotation at the magic angle. Methods for the proper alignment of all components are presented along with protocols for MAS PFG NMR experiments. Finally, first diffusion measurements of n‐hexane and benzene being adsorbed together in the metal‐organic framework MOF‐5 are presented.
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