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CuxO - TiO2 Composites (x=1, 2) Studied by X-ray Photoelectron Spectroscopy
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10.1116/11.20110101
/content/avs/journal/sss/16/1/10.1116/11.20110101
http://aip.metastore.ingenta.com/content/avs/journal/sss/16/1/10.1116/11.20110101

Figures

Image of Untitled

Accession# 01108–01
CuO-TiO nanocomposite
XPS
survey
Perkin-Elmer Physical Electronics, Inc. 5600ci
Al
1486.6 eV
250 W
>25 mm × >25 mm
spherical sector
45°
187.85 eV
1.9 eV
168.9 s
185.8 s
5
1.9 eV

Image of Untitled

  • •  01108–02
  • •  CuO-TiO nanocomposite
  • •  XPS
  • •  C 1
  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci
  • Excitation Source: Al
  • Source Energy: 1486.6 eV
  • Source Strength: 250 W
  • Source Size: >25 mm × >25 mm
  • Analyzer Type: spherical sector
  • Incident Angle: 9°
  • Emission Angle: 45°
  • Analyzer Pass Energy: 58.7 eV
  • Analyzer Resolution: 0.6 eV
  • Total Signal Accumulation Time: 80.4 s
  • Total Elapsed Time: 88.4 s
  • Number of Scans: 8
  • Effective Detector Width: 0.6 eV
  • Comment: See footnote below the Spectral Features Table.

Image of Untitled

  • •  01108–03
  • •  CuO-TiO nanocomposite
  • •  XPS
  • •  O 1
  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci
  • Excitation Source: Al
  • Source Energy: 1486.6 eV
  • Source Strength: 250 W
  • Source Size: >25 mm × >25 mm
  • Analyzer Type: spherical sector
  • Incident Angle: 9°
  • Emission Angle: 45°
  • Analyzer Pass Energy: 58.7 eV
  • Analyzer Resolution: 0.6 eV
  • Total Signal Accumulation Time: 80.4 s
  • Total Elapsed Time: 88.4 s
  • Number of Scans: 8
  • Effective Detector Width: 0.6 eV
  • Comment: See footnote below the Spectral Features Table.

Image of Untitled

  • •  01108–04
  • •  CuO-TiO nanocomposite
  • •  XPS
  • •  Cu 2
  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci
  • Excitation Source: Al
  • Source Energy: 1486.6 eV
  • Source Strength: 250 W
  • Source Size: >25 mm × >25 mm
  • Analyzer Type: spherical sector
  • Incident Angle: 9°
  • Emission Angle: 45°
  • Analyzer Pass Energy: 58.7 eV
  • Analyzer Resolution: 0.6 eV
  • Total Signal Accumulation Time: 400.8 s
  • Total Elapsed Time: 440.9 s
  • Number of Scans: 16
  • Effective Detector Width: 0.6 eV
  • Comment: See footnote below the Spectral Features Table.

Image of Untitled

  • •  01108–05
  • •  CuO-TiO nanocomposite
  • •  XPS
  • •  Ti 2
  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci
  • Excitation Source: Al
  • Source Energy: 1486.6 eV
  • Source Strength: 250 W
  • Source Size: >25 mm × >25 mm
  • Analyzer Type: spherical sector
  • Incident Angle: 9°
  • Emission Angle: 45°
  • Analyzer Pass Energy: 58.7 eV
  • Analyzer Resolution: 0.6 eV
  • Total Signal Accumulation Time: 100.4 s
  • Total Elapsed Time: 110.4 s
  • Number of Scans: 8
  • Effective Detector Width: 0.6 eV
  • Comment: The Ti 2p BE was 458.6 eV (FWHM=1.8 eV), as expected for Ti(IV) oxide (Refs. 37–41 ).

Image of Untitled

Accession# 01109–01
CuO-TiO nanocomposite
XPS
survey
Perkin-Elmer Physical Electronics, Inc. 5600ci
Al
1486.6 eV
250 W
>25 mm × >25 mm
spherical sector
45°
187.85 eV
1.9 eV
135.1 s
148.6 s
4
1.9 eV

Image of Untitled

  • •  01109–02
  • •  CuO-TiO nanocomposite
  • •  XPS
  • •  C 1
  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci
  • Excitation Source: Al
  • Source Energy: 1486.6 eV
  • Source Strength: 250 W
  • Source Size: >25 mm × >25 mm
  • Analyzer Type: spherical sector
  • Incident Angle: 9°
  • Emission Angle: 45°
  • Analyzer Pass Energy: 58.7 eV
  • Analyzer Resolution: 0.6 eV
  • Total Signal Accumulation Time: 80.4 s
  • Total Elapsed Time: 88.4 s
  • Number of Scans: 8
  • Effective Detector Width: 0.6 eV
  • Comment: See footnote below the Spectral Features Table.

Image of Untitled

  • •  01109–03
  • •  CuO-TiO nanocomposite
  • •  XPS
  • •  O 1
  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci
  • Excitation Source: Al
  • Source Energy: 1486.6 eV
  • Source Strength: 250 W
  • Source Size: >25 mm × >25 mm
  • Analyzer Type: spherical sector
  • Incident Angle: 9°
  • Emission Angle: 45°
  • Analyzer Pass Energy: 58.7 eV
  • Analyzer Resolution: 0.6 eV
  • Total Signal Accumulation Time: 80.4 s
  • Total Elapsed Time: 88.4 s
  • Number of Scans: 8
  • Effective Detector Width: 0.6 eV
  • Comment: See footnote below the Spectral Features Table.

Image of Untitled

  • •  01109–04
  • •  CuO-TiO nanocomposite
  • •  XPS
  • •  Cu 2
  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci
  • Excitation Source: Al
  • Source Energy: 1486.6 eV
  • Source Strength: 250 W
  • Source Size: >25 mm × >25 mm
  • Analyzer Type: spherical sector
  • Incident Angle: 9°
  • Emission Angle: 45°
  • Analyzer Pass Energy: 58.7 eV
  • Analyzer Resolution: 0.6 eV
  • Total Signal Accumulation Time: 400.8 s
  • Total Elapsed Time: 440.9 s
  • Number of Scans: 16
  • Effective Detector Width: 0.6 eV
  • Comment: See footnote below the Spectral Features Table.

Image of Untitled

  • •  01109–05
  • •  CuO-TiO nanocomposite
  • •  XPS
  • •  Ti 2
  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci
  • Excitation Source: Al
  • Source Energy: 1486.6 eV
  • Source Strength: 250 W
  • Source Size: >25 mm × >25 mm
  • Analyzer Type: spherical sector
  • Incident Angle: 9°
  • Emission Angle: 45°
  • Analyzer Pass Energy: 58.7 eV
  • Analyzer Resolution: 0.6 eV
  • Total Signal Accumulation Time: 100.4 s
  • Total Elapsed Time: 110.4 s
  • Number of Scans: 8
  • Effective Detector Width: 0.6 eV
  • Comment: The Ti 2p BE was 458.6 eV (FWHM=1.8 eV), as expected for Ti(IV) oxide (Refs. 37–41 ).

Tables

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SPECTRAL FEATURES TABLE

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ANALYZER CALIBRATION TABLE

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GUIDE TO FIGURES

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Generic image for table
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/content/avs/journal/sss/16/1/10.1116/11.20110101
2011-04-18
2014-04-23
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752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: CuxO - TiO2 Composites (x=1, 2) Studied by X-ray Photoelectron Spectroscopy
http://aip.metastore.ingenta.com/content/avs/journal/sss/16/1/10.1116/11.20110101
10.1116/11.20110101
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