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Beam damage of HS(CH2)15 COOH Terminated Self Assembled Monolayer (SAM) as Observed by X-ray Photoelectron Spectroscopy
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10.1116/11.20080601
/content/avs/journal/sss/18/1/10.1116/11.20080601
http://aip.metastore.ingenta.com/content/avs/journal/sss/18/1/10.1116/11.20080601

Figures

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Accession #01212–01Host MaterialHS(CH2) COOH terminated self-assembled monolayerTechniqueXPSSpectral RegionsurveyInstrumentPhysical Electronics, Incorporated Quantum 2000Excitation SourceAl K α monochromaticSource Energy1486.7 eVSource Strength99.3 WSource Size0.1 mm × 0.1 mmAnalyzer Typespherical sectorIncident AngleEmission Angle45°Analyzer Pass Energy:117.4 eVAnalyzer Resolution1.174 eVTotal Signal Accumulation Time437 sTotal Elapsed Time593 sNumber of Scans6Effective Detector Width1.174 eVCommentInitial wide scan spectra of the HS(CH_2)_15 COOH terminated self-assembled monolayer.

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Accession #01212–02Host MaterialHS(CH2) COOH terminated self-assembled monolayerTechniqueXPSSpectral RegionsurveyInstrumentPhysical Electronics, Incorporated Quantum 2000Excitation SourceAl K α monochromaticSource Energy1486.7 eVSource Strength99.3 WSource Size0.1 mm × 0.1 mmAnalyzer Typespherical sectorIncident AngleEmission Angle45°Analyzer Pass Energy:117.4 eVAnalyzer Resolution1.174 eVTotal Signal Accumulation Time437 sTotal Elapsed Time593 sNumber of Scans6Effective Detector Width1.174 eVCommentWide scan spectrum of HS(CH_2)_15 COOH terminated self-assembled monolayer after 231 minutes of x-ray beam exposure

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Accession #01212–03, 01212–07, 01212–11, 01212–15, 01212–19, 01212–23, 01212–27, 01212–31, 01212–35, 01212–39Host MaterialHS(CH2) COOH terminated self-assembled monolayerTechniqueXPSSpectral RegionC 1s InstrumentPhysical Electronics, Incorporated Quantum 2000Excitation SourceAl K α monochromaticSource Energy1486.7 eVSource Strength99.3 WSource Size0.1 mm × 0.1 mmAnalyzer Typespherical sectorIncident AngleEmission Angle45°Analyzer Pass Energy:46.95 eVAnalyzer Resolution0.4695 eVTotal Signal Accumulation Time209 sTotal Elapsed Time356 sNumber of Scans12Effective Detector Width0.4695 eVComment#01212-03: C 1s region cycle 1; #01212-07: C 1s region cycle 2; #01212-11: C 1s region cycle 3; #01212-15: C 1s region cycle 4; #01212-19: C 1s region cycle 5; #01212-23: C 1s region cycle 6; #01212-27: C 1s region cycle 7; #01212-31: C 1s region cycle 8; #01212-35: C 1s region cycle 9; #01212-39: C 1s region cycle 10

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Accession #01212–04, 01212–08, 01212–12, 01212–16, 01212–20, 01212–24, 01212–28, 01212–32, 01212–36, 01212–40Host MaterialHS(CH2) COOH terminated self-assembled monolayerTechniqueXPSSpectral RegionO 1s InstrumentPhysical Electronics, Incorporated Quantum 2000Excitation SourceAl K α monochromaticSource Energy1486.7 eVSource Strength99.3 WSource Size0.1 mm × 0.1 mmAnalyzer Typespherical sectorIncident AngleEmission Angle45°Analyzer Pass Energy46.95 eVAnalyzer Resolution0.4695 eVTotal Signal Accumulation Time209 sTotal Elapsed Time356 sNumber of Scans12Effective Detector Width0.4695 eVComment#01212-04: O 1s region cycle 1; #01212-08: O 1s region cycle 2; #01212-12: O 1s region cycle 3; #01212-16: O 1s region cycle 4; #01212-20: O 1s region cycle 5; #01212-24: O 1s region cycle 6; #01212-28: O 1s region cycle 7; #01212-32: O 1s region cycle 8; #01212-36: O 1s region cycle 9; #01212-40: O 1s region cycle 10

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Accession #01212–05, 01212–09, 01212–13, 01212–17, 01212–21, 01212–25, 01212–29, 01212–33, 01212–37, 01212–41Host MaterialHS(CH2) COOH terminated self-assembled monolayerTechniqueXPSSpectral RegionAu 4f InstrumentPhysical Electronics, Incorporated Quantum 2000Excitation SourceAl K α monochromaticSource Energy1486.7 eVSource Strength99.3 WSource Size0.1 mm × 0.1 mmAnalyzer Typespherical sectorIncident AngleEmission Angle45°Analyzer Pass Energy46.95 eVAnalyzer Resolution0.4695 eVTotal Signal Accumulation Time87 sTotal Elapsed Time141 sNumber of Scans4Effective Detector Width0.4695 eVComment#01212-05: Au 4f region cycle 1; #01212-09: Au 4f region cycle 2; #01212-13: Au 4f region cycle 3; #01212-17: Au 4f region cycle 4; #01212-21: Au 4f region cycle 5; #01212-25: Au 4f region cycle 6; #01212-29: Au 4f region cycle 7; #01212-33: Au 4f region cycle 8; #01212-37: Au 4f region cycle 9; #01212-41: Au 4f region cycle 10

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Accession #01212–06, 01212–10, 01212–14, 01212–18, 01212–22, 01212–26, 01212–30, 01212–34, 01212–38, 01212–42Host MaterialHS(CH2) COOH terminated self-assembled monolayerTechniqueXPSSpectral RegionS 2p InstrumentPhysical Electronics, Incorporated Quantum 2000Excitation SourceAl K α monochromaticSource Energy1486.7 eVSource Strength99.3 WSource Size0.1 mm × 0.1 mmAnalyzer Typespherical sectorIncident AngleEmission Angle45°Analyzer Pass Energy46.95 eVAnalyzer Resolution0.4695 eVTotal Signal Accumulation Time314 sTotal Elapsed Time535 sNumber of Scans18Effective Detector Width0.4695 eVComment#01212-06: S 2p region cycle 1; #01212-10: S 2p region cycle 2; #01212-14: S 2p region cycle 3; #01212-18: S 2p region cycle 4; #01212-22: S 2p region cycle 5; #01212-26: S 2p region cycle 6; #01212-30: S 2p region cycle 7; #01212-34: S 2p region cycle 8; #01212-38: S 2p region cycle 9; #01212-42: S 2p region cycle 10

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Tables

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SPECTRAL FEATURES TABLE

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ANALYZER CALIBRATION TABLE

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GUIDE TO FIGURES

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/content/avs/journal/sss/18/1/10.1116/11.20080601
2012-07-25
2014-04-21
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752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: Beam damage of HS(CH2)15 COOH Terminated Self Assembled Monolayer (SAM) as Observed by X-ray Photoelectron Spectroscopy
http://aip.metastore.ingenta.com/content/avs/journal/sss/18/1/10.1116/11.20080601
10.1116/11.20080601
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