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Ag/ZnO Nanocomposites Studied by X-ray Photoelectron Spectroscopy
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10.1116/11.20110902
/content/avs/journal/sss/18/1/10.1116/11.20110902
http://aip.metastore.ingenta.com/content/avs/journal/sss/18/1/10.1116/11.20110902

Figures

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Accession #01203–01Host MaterialAg/ZnO nanocompositeTechniqueXPSSpectral Regionsurvey InstrumentPerkin-Elmer Physical Electronics, Inc. 5600ciExcitation SourceMg K α Source Energy1253.6 eVSource Strength350 WSource Size>25 mm × >25 mmAnalyzer Typespherical sectorIncident AngleEmission Angle45°Analyzer Pass Energy:187.85 eVAnalyzer Resolution1.9 eVTotal Signal Accumulation Time110.1 sTotal Elapsed Time121.1 sNumber of Scans4Effective Detector Width1.9 eV

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  • Accession #:01203–02

  • Host Material: Ag/ZnO nanocomposite

  • Technique: XPS

  • Spectral Region: C 1s

  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci

  • Excitation Source: Mg K α

  • Source Energy: 1253.6 eV

  • Source Strength: 350 W

  • Source Size: >25 mm × >25 mm

  • Analyzer Type: spherical sector

  • Incident Angle: 9°

  • Emission Angle: 45°

  • Analyzer Pass Energy: 58.7 eV

  • Analyzer Resolution: 0.6 eV

  • Total Signal Accumulation Time: 30.1s

  • Total Elapsed Time: 33.2 s

  • Number of Scans: 3

  • Effective Detector Width: 0.6 eV

  • Comment: See footnote below the Spectral Features Table.

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  • Accession #:01203–03

  • Host Material: Ag/ZnO nanocomposite

  • Technique: XPS

  • Spectral Region: O 1s

  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci

  • Excitation Source: Mg K α

  • Source Energy: 1253.6 eV

  • Source Strength: 350 W

  • Source Size: >25 mm × >25 mm

  • Analyzer Type: spherical sector

  • Incident Angle: 9°

  • Emission Angle: 45°

  • Analyzer Pass Energy: 58.7 eV

  • Analyzer Resolution: 0.6 eV

  • Total Signal Accumulation Time: 30.1 s

  • Total Elapsed Time: 33.2 s

  • Number of Scans: 3

  • Effective Detector Width: 0.6 eV

  • Comment: See footnote below the Spectral Features Table.

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  • Accession #:01203–04

  • Host Material: Ag/ZnO nanocomposite

  • Technique: XPS

  • Spectral Region: Zn 3p

  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci

  • Excitation Source: Mg K α

  • Source Energy: 1253.6 eV

  • Source Strength: 350 W

  • Source Size: >25 mm × >25 mm

  • Analyzer Type: spherical sector

  • Incident Angle: 9°

  • Emission Angle: 45°

  • Analyzer Pass Energy: 58.7 eV

  • Analyzer Resolution: 0.6 eV

  • Total Signal Accumulation Time: 30.1 s

  • Total Elapsed Time: 33.2 s

  • Number of Scans: 3

  • Effective Detector Width: 0.6 eV

  • Comment: See footnote below the Spectral Features Table.

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  • Accession #:01203–05

  • Host Material: Ag/ZnO nanocomposite

  • Technique: XPS

  • Spectral Region: Zn 2p3/2

  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci

  • Excitation Source: Mg K α

  • Source Energy: 1253.6 eV

  • Source Strength: 350 W

  • Source Size: >25 mm × >25 mm

  • Analyzer Type: spherical sector

  • Incident Angle: 9°

  • Emission Angle: 45°

  • Analyzer Pass Energy: 58.7 eV

  • Analyzer Resolution: 0.6 eV

  • Total Signal Accumulation Time: 30.1s

  • Total Elapsed Time: 33.2 s

  • Number of Scans: 3

  • Effective Detector Width: 0.6 eV

  • Comment: See footnote below the Spectral Features Table.

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  • Accession #:01203–06

  • Host Material: Ag/ZnO nanocomposite

  • Technique: XPS

  • Spectral Region: Zn LMM

  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci

  • Excitation Source: Mg K α

  • Source Energy: 1253.6 eV

  • Source Strength: 350 W

  • Source Size: >25 mm × >25 mm

  • Analyzer Type: spherical sector

  • Incident Angle: 9°

  • Emission Angle: 45°

  • Analyzer Pass Energy: 58.7 eV

  • Analyzer Resolution: 0.6 eV

  • Total Signal Accumulation Time: 37.7 s

  • Total Elapsed Time: 41.4 s

  • Number of Scans: 3

  • Effective Detector Width: 0.6 eV

  • Comment: See comment to Accession #1203-05. The KE of the Zn LMM signal was calculated using the most intense Auger peak component.

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  • Accession #:01203–07

  • Host Material: Ag/ZnO nanocomposite

  • Technique: XPS

  • Spectral Region: Ag 3d

  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci

  • Excitation Source: Mg K α

  • Source Energy: 1253.6 eV

  • Source Strength: 350 W

  • Source Size: >25 mm × >25 mm

  • Analyzer Type: spherical sector

  • Incident Angle: 9°

  • Emission Angle: 45°

  • Analyzer Pass Energy: 58.7 eV

  • Analyzer Resolution: 0.6 eV

  • Total Signal Accumulation Time: 30.1 s

  • Total Elapsed Time: 33.2 s

  • Number of Scans: 3

  • Effective Detector Width: 0.6 eV

  • Comment: See footnote below the Spectral Features Table.

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  • Accession #:01203–08

  • Host Material: Ag/ZnO nanocomposite

  • Technique: XPS

  • Spectral Region: Ag MVV

  • Instrument: Perkin-Elmer Physical Electronics, Inc. 5600ci

  • Excitation Source: Mg K α

  • Source Energy: 1253.6 eV

  • Source Strength: 350 W

  • Source Size: >25 mm × >25 mm

  • Analyzer Type: spherical sector

  • Incident Angle: 9°

  • Emission Angle: 45°

  • Analyzer Pass Energy: 58.7 eV

  • Analyzer Resolution: 0.6 eV

  • Total Signal Accumulation Time: 60.1 s

  • Total Elapsed Time: 66.2 s

  • Number of Scans: 3

  • Effective Detector Width: 0.6 eV

  • Comment: See footnote below the Spectral Features Table.

Tables

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SPECTRAL FEATURES TABLE

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ANALYZER CALIBRATION TABLE

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GUIDE TO FIGURES

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/content/avs/journal/sss/18/1/10.1116/11.20110902
2012-03-16
2014-04-17
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752b84549af89a08dbdd7fdb8b9568b5 journal.articlezxybnytfddd
Scitation: Ag/ZnO Nanocomposites Studied by X-ray Photoelectron Spectroscopy
http://aip.metastore.ingenta.com/content/avs/journal/sss/18/1/10.1116/11.20110902
10.1116/11.20110902
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