Dynamic force microscopy by means of the phase-controlled oscillator method
J. Appl. Phys. 82, 3641 (1997); doi:10.1063/1.365726
Issue Date: 15 October 1997
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Dynamic force microscopy, a technique also known as non-contact force microscopy, has proved to be a powerful tool for atomic resolution imaging. A number of schemes have been developed, but recently the oscillator method has become the preferred operating mode. Here, the force sensor acts as resonator in an active feedback circuit. A practical implementation of the method is described and the underlying key concepts are discussed. It is shown that a tracking oscillator excitation scheme is superior to the more standard direct feedback method for cases in which the force sensor exhibits only a weak resonance enhancement. Furthermore, the simultaneous measurement of dissipative interaction channels is an important extension of dynamic force microscopy. It allows one to differentiate between sample materials via their plasto-mechanical response. As an example, a Cr test grating has been imaged in the constant force gradient mode. The dissipation measured on Cr-covered areas is significantly lower than that on the bare quartz glass substrate, which enables one to distinguish between the two materials with a lateral resolution comparable to that of the topographic image. ©1997 American Institute of Physics.
| History: | Received 3 June 1997; accepted 15 July 1997 |
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http://link.aip.org/link/?JAPIAU/82/3641/1 |
KEYWORDS and PACS
- 07.79.Lh
Instruments, apparatus, components, and techniques common to several branches of physics and astronomy Scanning probe microscopes, components, and techniques Atomic force microscopes - 84.30.Ng
Electronics: radiowave and microwave technology; direct energy conversion and storage Electronic circuits Oscillators, pulse generators, and function generators - 61.16.Ch
Structure of solids and liquids; crystallography Electron, ion, and scanning probe microscopy Scanning probe microscopy: scanning tunneling, atomic force, scanning optical, magnetic force, etc. - YEAR: 1996-97
PUBLICATION DATA
0021-8979 (print)
1089-7550 (online)
REFERENCES (19)
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- G. Binning, H. Rohrer, Ch. Gerber, and E. Weibel, Phys. Rev. Lett. 49, 57 (1982);
- G. Binning, C. F. Quate, and C. Gerber, Phys. Rev. Lett. 56, 930 (1986);
- U. Dürig, J. K. Gimzewski, and D. W. Pohl, Phys. Rev. Lett. 57, 2403 (1986).
- U. Dürig, O. Züger, and A. Stalder, J. Appl. Phys. 72, 1778 (1992).
- W. Denk and D. W. Pohl, Appl. Phys. Lett. 59, 2171 (1991).
- P. Grütter, Y. Liu, P. LeBlanc, and U. Dürig, Appl. Phys. Lett. 71, 279 (1997).
- F. J. Giessibl,
Science 267, 68 (1995) . - Y. Sugawara, M. Ohta, H. Ueyama, S. Morita, F. Osaka, S. Ohkouchi, M. Suzuki, and S. Mishima,
J. Vac. Sci. Technol. B 14, 953 (1996) . - R. Lüthi, E. Meyer, M. Bammerlin, A. Baratoff, T. Lehmann, L. Howald, Ch. Gerber, and H.-J. Güntherodt,
Z. Phys. B 100, 165 (1996) . - U. Dürig and O. Züger, Phys. Rev. B 50, 5008 (1994).
- T. R. Albrecht, P. Grütter, D. Horne, and D. Rugar, J. Appl. Phys. 69, 668 (1991).
- See, e.g., D. Sarid, in Ref. 2, Chap. 2, pp. 1938.
- See Eqs. (16) and (35) in Ref. 4.
- For details see, e.g., U. Tietze and Ch. Schenk, Halbleiter-Schaltungstechnik, 4th ed., (Springer, Berlin, 1978), Chap. 26.
- See Fig. 13 and Eq. (33) in Ref. 4.
- N. Blanc, J. Brugger, N. F. de Rooij, and U. Dürig,
J. Vac. Sci. Technol. B 14, 901 (1996) . - M. W. Putty, M. S. thesis, University of Michigan at Ann Arbor, 1988.
- The actual interaction force gradient
F is of the order of
x/
larger than the mean force gradient because the tip senses the interaction only during a short period of the order of the interaction length
divided by the vibration amplitude
x. With the force given by
F ×
one infers that the tapping force is of the order of the vibration amplitude times the mean force gradient. - H. Yoshizawa, Y.-L. Chen, and J. Israelachvili,
J. Phys. Chem. 97, 4128 (1993) .






