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Sintering and crystallization behavior of CaMgSi2O6–NaFeSi2O6 based glass-ceramics

J. Appl. Phys. 106, 093502 (2009); doi:10.1063/1.3239852

Published 4 November 2009

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Ashutosh Goel,1,2 Anna Maria Ferrari,3 Ishu Kansal,1,2 Maria J. Pascual,4 Luisa Barbieri,2 Federica Bondioli,2 Isabella Lancellotti,2 Manuel J. Ribeiro,5 and José M. F. Ferreira1
1Department of Ceramics and Glass Engineering, CICECO, University of Aveiro, 3810-193 Aveiro, Portugal
2Dipartimento di Ingegneria dei Materiali e dell'Ambiente, Facoltà di Ingegneria, Universitá di Modena e Reggio Emilia, 41100 Modena, Italy
3Dipartimento di Scienze e Metodi dell'Ingegneria, Facoltà di Ingegneria, Universitdiá Modena e Reggio Emilia, 42100 Reggio Emilia, Italy
4Instituto de Cerámica y Vidrio, CSIC, Kelsen 5, Campus de Cantoblanco, 28049 Madrid, Spain
5UIDM, ESTG, Polytechnic Institute of Viana do Castelo, 4900 Viana do Castelo, Portugal
We report on the synthesis, sintering, and crystallization behaviors of a glass with a composition corresponding to 90  mol %  CaMgSi2O6−10  mol %  NaFeSi2O6. The investigated glass composition crystallized superficially immediately after casting of the melt and needs a high cooling rate (rapid quenching) in order to produce an amorphous glass. Differential thermal analysis and hot-stage microscopy were employed to investigate the glass forming ability, sintering behavior, relative nucleation rate, and crystallization behavior of the glass composition. The crystalline phase assemblage in the glass-ceramics was studied under nonisothermal heating conditions in the temperature range of 850–950 °C in both air and N2 atmosphere. X-ray diffraction studies adjoined with the Rietveld–reference intensity ratio method were employed to quantify the amount of crystalline phases, while electron microscopy was used to shed some light on the microstructure of the resultant glass-ceramics. Well sintered glass-ceramics with diopside as the primary crystalline phase were obtained where the amount of diopside varied with the heating conditions. ©2009 American Institute of Physics
History: Received 5 June 2009; accepted 31 August 2009; published 4 November 2009
Permalink: http://link.aip.org/link/?JAPIAU/106/093502/1
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KEYWORDS and PACS

Keywords
PACS
  • 81.05.Pj
    Glass-based composites, vitroceramics: fabrication, treatment, testing and analysis
  • 64.70.kj
    Solid-solid transitions in glasses
  • YEAR: 2009

PUBLICATION DATA

ISSN:
0021-8979 (print)   1089-7550 (online)
Publisher:
AIP is a member of CrossRef AIP

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