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Chemical shift scaling in NMR of rotating solids

J. Chem. Phys. 75, 5594 (1981); doi:10.1063/1.441996

Issue Date: 15 December 1981

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J. A. DiVerdi and S. J. Opella
Department of Chemistry, University of Pennsylvania, Philadelphia, Pennsylvania 19104
An improved version of the chemical shift scaling multipulse cycle is demonstrated that eliminates the dependence of the direction of the axis of precession on the extent of scaling. This prevents the formation of a zero-frequency artifact in the final spectrum. Results from liquid, as well as stationary and spinning solid samples, are described. The Journal of Chemical Physics is copyrighted by The American Institute of Physics.
Permalink: http://link.aip.org/link/?JCPSA6/75/5594/1
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KEYWORDS and PACS

Keywords
PACS
  • 76.60.Cq
    Magnetic resonances and relaxation in condensed matter; Mössbauer effect Nuclear magnetic resonance and relaxation Chemical and Knight shifts
  • YEAR: 1981

PUBLICATION DATA

ISSN:
0021-9606 (print)   1089-7690 (online)
Publisher:
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REFERENCES (4)
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  1. U. Haeberlen and J. S. Waugh, Phys. Rev. 175, 453 (1968).
  2. J. D. Ellett and J. S. Waugh, J. Chem. Phys. 51, 2851 (1969).
  3. U. Haeberlen, J. D. Ellett, and J. S. Waugh, J. Chem. Phys. 55, 53 (1971).
  4. J. A. DiVerdi and S. J. Opella (unpublished).

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