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Automated gas burette system for evolved hydrogen measurements

Rev. Sci. Instrum. 79, 084103 (2008); doi:10.1063/1.2968715

Published 14 August 2008

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Feng Zheng, Scot D. Rassat, David J. Helderandt, Dustin D. Caldwell, Christopher L. Aardahl, Tom Autrey, John C. Linehan, and Kenneth G. Rappé
Pacific Northwest National Laboratory, P.O. Box 999, Richland, Washington 99352, USA
This paper reports a simple and efficient gas burette system that allows automated determination of evolved gas volume in real time using only temperature and pressure measurements. The system is reliable and has been used successfully to study the hydrogen release kinetics of ammonia borane thermolysis. The system is especially suitable for bench scale studies involving small batches and potentially rapid reaction kinetics. ©2008 American Institute of Physics
History: Received 2 June 2008; accepted 17 July 2008; published 14 August 2008
Permalink: http://link.aip.org/link/?RSINAK/79/084103/1

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KEYWORDS and PACS

Keywords
PACS
  • 84.60.-h
    Direct energy conversion and energy storage
  • 06.30.-k
    Measurements common to several branches of physics and astronomy
  • YEAR: 2008

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PUBLICATION DATA

ISSN:
0034-6748 (print)   1089-7623 (online)
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