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Experimental method for in situ determination of material textures at simultaneous high pressure and high temperature by means of radial diffraction in the diamond anvil cell

Rev. Sci. Instrum. 80, 104501 (2009); doi:10.1063/1.3236365

Published 13 October 2009

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Hanns-Peter Liermann,1,2 Sébastien Merkel,3 Lowell Miyagi,4 Hans-Rudolf Wenk,4 Guoyin Shen,1 Hyunchae Cynn,5 and William J. Evans5
1High-Pressure Collaboration Access Team, Geophysical Laboratory, Carnegie Institution of Washington, Argonne, Illinois 60439, USA
2DESY, Hamburg 22607, Germany
3Laboratoire de Structure et Propriétés de l'Etat Solide, Université Lille1, CNRS, 59655 Villeneuve d'Ascq Cedex, France
4Department of Earth and Planetary Science, University of California-Berkeley, California 94720, USA
5High Pressure Physics Group, Lawrence Livermore National Laboratory, 7000 East Avenue, L-041 Livermore, California 94550, USA
We introduce the design and capabilities of a resistive heated diamond anvil cell that can be used for side diffraction at simultaneous high pressure and high temperature. The device can be used to study lattice-preferred orientations in polycrystalline samples up to temperatures of 1100 K and pressures of 36 GPa. Capabilities of the instrument are demonstrated with preliminary results on the development of textures in the bcc, fcc, and hcp polymorphs of iron during a nonhydrostatic compression experiment at simultaneous high pressure and high temperature. ©2009 American Institute of Physics
History: Received 23 June 2009; accepted 1 September 2009; published 13 October 2009
Permalink: http://link.aip.org/link/?RSINAK/80/104501/1
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KEYWORDS and PACS

Keywords
PACS
  • 07.35.+k
    High-pressure apparatus; shock tubes; diamond anvil cells
  • 06.30.-k
    Measurements common to several branches of physics and astronomy
  • 07.20.Ka
    High-temperature instrumentation; pyrometers
  • 81.70.-q
    Methods of materials testing and analysis
  • YEAR: 2009

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PUBLICATION DATA

ISSN:
0034-6748 (print)   1089-7623 (online)
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